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While the use of voltammetric techniques have
often been suggested to analyze pesticides in general,
only a small number of methods are available for the
determination of imidacloprid [34–36] and, to the best
of our knowledge, no publications dealing with the
electroanalytical determination of thiamethoxam appeared
so far.
In our previous work we reported on the determination
of substances thiamethoxam and imidacloprid
with linear sweep voltammetry (LSV) on a glassy
carbon electrode [37] at a ppm concentration level.
As a continuation of our previous study, the aim of
the present work was to investigate the polarographic
behavior of thiamethoxam and to elaborate a rapid,
simple and sufficiently sensitive (ppb concentration
level) DPP method for the determination of this compound
in commercial formulations of thiamethoxam,
as well as in thiamethoxam treated potato and maize
samples.

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