UC知道请帮忙翻译一下有机化学实验英文资料，最好详细点。
来源：百度知道 编辑：UC知道 时间：2024/05/30 07:13:44
A mixture of the ketone (10 mmol), titanium(IV) isopropoxide(6.0 mL, 20 mmol) and ammonia in ethyl alcohol(2 M, 25 mL, 50 mmol) was stirred under argon in a capped flask at ambient temperature for 6 h.
Sodium borohydride(0.6 g, 15 mmol) was then added and the resulting mixture was stirred at room temperature for an additional 3 h.
The reaction was then quenched by pouring into ammonium hydroxide (2 M, 25 mL), the resulting inorganic precipitate was filtered off, and washed with ethyl acetate (25 mL￡2).
The organic layer was separated and the remaining aqueous layer was extracted with ethyl acetate (25 mL￡2).
The combined organic solution was next extracted with hydrochloric acid (1 M, 30 mL) to separate the neutral materials.
The acidic aqueous extracts were washed with ethyl acetate (50 mL), then treated with aqueous sodium hydroxide (2 M) to pH 10–12, and extracted with ethyl acetate (50 mL￡3).
The combined organic extracts were washed with brine (50
Sodium borohydride(0.6 g, 15 mmol) was then added and the resulting mixture was stirred at room temperature for an additional 3 h.
The reaction was then quenched by pouring into ammonium hydroxide (2 M, 25 mL), the resulting inorganic precipitate was filtered off, and washed with ethyl acetate (25 mL￡2).
The organic layer was separated and the remaining aqueous layer was extracted with ethyl acetate (25 mL￡2).
The combined organic solution was next extracted with hydrochloric acid (1 M, 30 mL) to separate the neutral materials.
The acidic aqueous extracts were washed with ethyl acetate (50 mL), then treated with aqueous sodium hydroxide (2 M) to pH 10–12, and extracted with ethyl acetate (50 mL￡3).
The combined organic extracts were washed with brine (50
我是按照实验步骤的习惯意译的，不是完全直译的，不过关键的东西都是直译的。
将酮（10毫摩尔,没说是什么酮啊……），异丙醇钛(IV)(6毫升，20毫摩尔)和氨的乙醇溶液（2摩尔/升，25毫升，50毫摩尔）置于具塞烧瓶中混合，在氩气气氛下搅拌,常温下反应6小时。
加入硼氢化钠（0.6g，15毫摩尔）在反应后的混合物中，室温下再搅拌反应3小时。
然后加入氨水（2摩尔/升，25毫升）中止反应，将得到的无机沉淀滤出，并用乙酸乙酯洗涤（25mL两次）。分离出有机层，剩下的水层加入乙酸乙酯萃取（25mL两次）。
将有机层合并，用盐酸（1摩尔/L，30毫升）萃取分离掉中性材料。
将酸性水层用乙酸乙酯（50毫升）洗涤，然后用硼氢化钠溶液（2摩尔/升）调节至pH 10~12，再用乙酸乙酯萃取（50毫升三次）。
合并有机层，用盐水（50毫升）洗涤后，加入干燥剂干燥（硫酸钠），然后真空干燥，得到对应的伯胺。